Introduction to Non-Destructive Testing TechniquesLiquid Penetrant TestingPage 9of 20The radius of the flaw or the distance between the flaw walls. The density or specific gravity of the penetrant. Microstructural properties of the penetrant. The ideal dwell time is often determined by experimentation and is often very specific to a particular application. For example, the table shows the dwell time requirements for steel parts according to some of the commonly used specifications. Penetrant Removal ProcessThe penetrant removal procedure must effectively remove the penetrant from the surface of the part without removing an appreciable amount of entrapped penetrant from the discontinuity. If the removal process extracts penetrant from the flaw, the flaw indication will be reduced by a proportional amount. If the penetrant is not effectively removed from the part surface, the contrast between the indication and the background will be reduced. Removal MethodAs mentioned previously, penetrant systems are classified into fourtypes according to the method used forexcess penetrant removal. -Method A: Water-Washable -Method B: Post-Emulsifiable, Lipophilic -Method C: Solvent Removable Introduction to Non-Destructive Testing TechniquesLiquid Penetrant TestingPage 10of 20-Method D: Post-Emulsifiable, Hydrophilic Method C, Solvent Removable, is used primarily for inspecting small localized areas. Phương pháp này đòi hỏi tay lau bề mặt với một Vải ẩm với dung môiBộ tháo gỡ và là, do đó,quá lao động chuyên sâuĐối với hầu hết các trường hợp sản xuất. Phương pháp A, nước-Có thể giặt, là các tiết kiệm nhấtđể áp dụngof các khác nhauphương phápvà nó rất dễ dàng sử dụng. Nước-có thể giặt hoặc tự-emulsifiable penetrants chứa một emulsifier là một phần của các xây dựng. Thấu dư thừa có thể loại bỏ từ sur đối tượngphải đối mặt với một đơn giản nước rửa.Khi loại bỏ các thấu từ các khiếm khuyết do trên-rửa phía là một mối quan tâm, một bài đăng-Hệ thống thẩm thấu emulsifiable có thể được sử dụng.Các pOST-emulsifiable phương pháp chỉ thường được dùng khi rất cao độ nhạy là cần thiết.Bài viết-emulsifiable penetrants yêu cầu một emulsifier riêng biệtđể phân tích thấu và làm cho nó nước có thể giặt. Phần là thường đắm mìnhở emulsifier nhưng Purifying emulsifiers cũng có thể được phun lên các đối tượng. Đánh răng emulsifier vào phần là không được khuyến cáo hoặc vì lông bàn chải có thể ép buộc emulsifier vào discontinuities, gây ra thấu entrapped được gỡ bỏ. Emulsifier là Tất cảnợ đủ thời gian để phản ứng với thấu trên bề mặtphần phía nhưng không thời gian nhất định để thực hiện theo cách của mình vào Khuyết tậtđể phản ứng với thấu bị mắc kẹt. Kiểm soát thời gian phản ứng là điều cần thiết quan trọng khi sử dụng một bài đăng-emulsifiable Hệ thống.If the emulsification time is too short, an excessive amount of penetrant will be left on the surface, leading to high background levels. If the emulsification time is too long, the emulsifier will react with the penetrant entrapped in discontinuities, making it possible to deplete the amount needed to form an indication. The hydrophilic post-emulsifiable method (Method D) is more sensitivethan the lipophilic post-emulsifiable method (Method B). The major advantageof hydrophilic emulsifiers is that theyare less sensitive to variation in the contact and removal time. When using an emulsifiable penetrant is used, the penetrant inspection process includes the following steps (extra steps are underlined): 1. pre-clean part, 2. apply penetrant and allow to dwell, 3.pre-rinse to remove first layer of penetrant, 4.apply hydrophilic emulsifier and allow contact for specified time, 5. rinse to remove excess penetrant, 6. dry part, 7. apply developer and allow part to develop, and 8. inspect.Rinse Method and Time for Water-Washable PenetrantsThe method used to rinse the excess penetrant from the object surface and the time of the rinse should be controlled so as to prevent over-washing. It is generally Introduction to Non-Destructive Testing TechniquesLiquid Penetrant TestingPage 11of 20recommended that a coarse spray rinse or an air-agitated,immersion wash tankbe used. When a sprayis being used, it should be directed at a 45° angle to the part surface so as to not force water directly into any discontinuities that may be present. The spray or immersion time should be kept to a minimum through frequent inspections of the remaining background level. Hand Wiping of Solvent Removable Penetrants When a solvent removable penetrant is used, care must also be taken to carefully remove the penetrant from the part surface while removing as little aspossible from the flaw. The first step in this cleaning procedure is to dry wipethe surface of the part in one directionusing a white, lint-free, cotton rag. One dry pass in one direction is all that should be used to remove as much penetrant as possible. Next, the surface should be wiped with one pass in one direction with a rag moistened with cleaner. One dry pass followed by one damp passis all that is recommended. Additional wiping may sometimes be necessary; but keep in mind that with every additional wipe, some of the entrapped penetrant will be removed and inspection sensitivity will be reduced. Use and Selection of a DeveloperThe use of developer is almost always recommended. The output from a fluorescent penetrant is improved significantlywhen a suitable powder developer isused. Also, the use of developer can have a dramatic effect on the probability of detectionof an inspection.Nonaqueous developers are generally recognized as the most sensitivewhen properly applied. However, if the thickness of the coating becomes too great, defects can be masked. The relative sensitivities of developers and application techniques as rankedin Volume II of the Nondestructive Testing Handbookare shown in the table below. Ranking12345678910Developer FormNonaqueous, Wet SolventPlastic FilmWater-SolubleWater-SuspendableWater-SolubleWater-SuspendableDryDryDryDryMethod of ApplicationSpraySpraySpraySprayImmersionImmersionDust Cloud (Electrostatic)Fluidized BedDust Cloud (Air Agitation)Immersion (Dip) Introduction to Non-Destructive Testing TechniquesLiquid Penetrant TestingPage 12of 20The following table lists the main advantages and disadvantages of the various developer types.DeveloperAdvantagesDisadvantagesDryIndications tend to remain brighter and more distinct over timeEasily to applyDoes not form contrast background so cannot be used with visible systemsDifficult to assure entire part surface has been coatedSolubleEase of coating entire part White coating for good contrast can be produced which work well for both visible and fluorescent systems Coating is translucent and provides poor contrast (not recommended for visual systems)Indications for water washable systems are dim and blurredSuspendableEase of coating entire part Indications are bright and sharpWhite coating for good contrast can be produced which work well for both visible and fluorescent systems Indications weaken and become diffused after timeNonaqueousVery portableEasy to apply to readily accessible surfaces White coating for good contrast can be produced which work well for both visible and fluorescent systems Indications show-up rapidly and are well defined Provides highest sensitivityDifficult to apply evenly to all surfacesMore difficult to clean part after inspectionIntroduction to Non-Destructive Testing TechniquesLiquid Penetrant TestingPage 13of 20Quality& ProcessControlQuality control of the penetrant inspection processis essentialto get good and consistentresults. Since several steps and materials are involved in the inspection process, there are quality control procedures for each of them.Temperature ControlThe temperature of the penetrant materials and the part being inspected can have an effect on the results. Temperatures from 27 to 49°C are reported in the literature to produce optimal results. Many specifications allow testing in the rangeof 4 to 52°C. Raising the temperature beyond this level will significantlyraise the speed of evaporation of penetrantscausing them to dry out quickly.Since the surface tension of most materials decrease as the temperature increases, raising the temperature of the penetrant will increase the wetting of the surface and the capillary forces. Of course, the opposite is also true, so lowering the temperature will have a negative effect on the flow characteristics.Penetrant Quality ControlThe quality of a penetrant inspection is highly dependent on the quality of the penetrant materials used. Only products meeting the requirements of an industry specification, such as AMS 2644, should be used. Deterioration of new penetrants primarily results from aging and contamination. Virtually all organic dyes deteriorate over time, resulting in a loss of color or fluorescent response, but deterioration can be slowed with proper storage. When possible, keep the materials in a closed container and protect from freezing and exposure to high heat. Contamination canoccur during storage and use. Of course, open tank systems are much more susceptible to contamination than are spray systems. Regular checks must be performed to ensure that the material performance has not degraded. When the penetrant is first received from the manufacturer, a sample of the fresh solution should be collected and stored as a standard for future comparison. The standard specimen should be stored in a sealed, opaque glass or metal contain
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