2. hóa chất cần thiết 1. 1/3 chén nitrat amoni (có được bằng cách cắt mở lạnh gói. Đó là các quả bóng màu trắng nhỏ. Hãy cẩn thận những gì bạn mua, một số gói lạnh nitrat amoni miễn phí. Ngoài ra, bạn đôi khi có thể tìm thấy các amoniac nitrat prills tại các cửa hàng hydroponics được bán như một số lượng lớn phân bón. 2. 1/2 chén 100% dung dịch kiềm (aka natri hydroxit. Có sẵn tại cửa hàng phần cứng trong phần dọn dẹp cống. -Tinh thể Drano, hoặc bất kỳ khác bột lye công trình) 3. 3 chén Coleman Camp nhiên liệu (động cơ bắt đầu từ chất lỏng [dietyl ete] hoặc naphtha VM & P cũng có thể được sử dụng) 4. 3 x Lithium dải (nhận bằng cách cắt mở Energizer AA Lithium pin - tìm kiếm YouTube cho - nhận được kim loại từ một Energizer Pin Lithium 5. 100ml NP dung môi của bạn lựa chọn (Xylen hoặc MEK khuyến cáo - dễ dàng tìm thấy tại cửa hàng phần cứng địa phương của bạn trong phần sơn) 6. 3-4 hộp 120mg 12-giờ pseudoephedrine HCl (PSE). Số lượng cao nhất, bạn có thể tìm thấy. (Sudafed hoặc một tương đương chung. HÃY CHẮC CHẮN RẰNG PSE LÀ PHẦN CHỈ HOẠT ĐỘNG.) 7. khoảng 1/3 chén iốt muối 8. 4 capfuls axít sulfuric (có sẵn như là chất lỏng cống sạch.) HAY axít muriatic (cũng được bán tại các cửa hàng phần cứng thường được tìm thấy xung quanh phần sơn) 9. Denatured rượu hay rượu Isopropyl 99% 10. 1/8 chén nước cất (mùa xuân Ba Lan hoặc bất kỳ nước đóng chai có thể cũng được sử dụng) 3. Preparation 1. Take the 20oz lid and cut a hole in it big enough to fit the aquarium tubing. It should be snug. 2. Cut one of the 2-liters in half. Discard the top. 3. Crush the pills into a fine powder. Use a coffee grinder, blender, or if worse comes to worse, hand crush them with a pair of pliers or something. Put the powder into a baggie. The beauty of "shake n bake" is you don't have to clean your pills to extract PSE. Just crush and toss in! 4. Measure out and crush the ammonium nitrate (optional). If it is dry enough, go ahead and crush it. Not important that you do this, though. It helps ensure even cooking, but is not imperative. Put it in a baggie. (ammonia nitrate is extremely hygroscopic once crushed) 5. Measure out the lye. Be careful not to touch this stuff. It eats anything organic (YOU included) and also reacts with metal. Put in a baggie. 6. Measure out the Coleman fuel or Naphtha. Put it into the 1-liter. 7. Cut open the batteries. You must do this quickly because lithium reacts with moisture in air and will become hot, possibly catching fire if it is very humid outside. Use the pipecutter to cut the outer housing of the battery. Use the needle nosed pliers to peel down the housing to expose the strip. There will be a black strip in between 2 pieces of paper. This is the one you want. BE CAREFUL. LITHIUM STRIPS MAKE A SPARK WHEN THEY COME INTO CONTACT WITH METAL. DO NOT TOUCH THE STRIP WITH YOUR BARE HANDS IF YOU CAN AVOID IT. DO NOT GET IT WET!!!!! Once you get the strip out of the battery, it can be stored in denatured alcohol, and will no longer react with air as long as it is capped. Lithium strips burn VIOLENTLY when they come into contact with water. Be CAREFUL!! Here is the how-to video again YouTube - Get Lithium Metal From an Energizer Battery 4. It's go time 1. Pour the ammonium nitrate into the 2-liter bottle (the one you didnt cut in half). 2. Add crushed pills. Shake up to mix them together. 3. Add your 100ml Xylene or MEK solvent At this point, you will see the ingredients starting to react, it will produce bubbles in the bottom. 4. Add the lithium strips. Take them out of the denatured alcohol, tear them into smaller pieces, and add them to the mixture. 5. Add your lye MAKING SURE to cover your Lithium strips. 6. Add the 1/4 cup of water. The water kicks off the reaction, but YOU MUST GET THE CAP ON IMMEDIATELY AFTER ADDING THE WATER. Remember Lithium reacts intensely with water and is potentially dangerous. The lithium-water reaction at normal temperatures is brisk but not violent, though the hydrogen produced can ignite. Do not add the water if your Lithium has not been buried and is UNDER YOUR LYE. 7. Add the Coleman fuel or Naphtha to this mixture. The mixture will be rolling now (it will look like it's boiling real hard). NOW THIS IS THE TRICKY AND MOST IMPORTANT PART: The reaction builds up necessary pressure inside the bottle, don't worry - you will need to let this react WITH THE CAP ON for at least 2 minutes. Let the Lithium do it's thing for a full 120 seconds. Venting or releasing pressure within the first 2-3 minutes will greatly affect your final yield. After 2 or 3 minutes you will see the Lithium starting to get smaller, shriveling up into small Bronze foil looking balls with holes throughout. This is when you MUST VENT by slightly unscrewing the cap to release the gas. ***AFTER THE LITHIUM TURNS BRONZE MAKE SURE TO KEEP AN EYE ON THE PRESSURE INSIDE THE BOTTLE! IT CAN EASILY BUILD UP QUICKLY AND EXPLODE IF NOT VENTED PROPERLY!*** You can gently swirl (not shake!) the bottle side-to-side if you want, you don't have to. Swirling can only help the reaction. Be careful! The gas coming out of t
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